A Hands-on Problem-Based NMR Experiment using a Benchtop Spectrometer for the Undergraduate Laboratory Supplementary Information (SI)

Jonathan Wong¹, Houguang Jeremy Chen¹, Ai-Hua Seow¹, Susanne D. Riegel^2, and Sumod A. Pullarkat^1,

¹Division of Chemistry and Biological Chemistry, School of Physical & Mathematical Sciences, Nanyang Technological University, Singapore 637371, Singapore

²Application Chemistry, Nanalysis Corp., Calgary, Alberta, Canada

Cite this paper:
Jonathan Wong, Houguang Jeremy Chen, Ai-Hua Seow, Susanne D. Riegel and Sumod A. Pullarkat. A Hands-on Problem-Based NMR Experiment using a Benchtop Spectrometer for the Undergraduate Laboratory Supplementary Information (SI). World Journal of Chemical Education. 2016; 4(3):52-63. doi: 10.12691/wjce-4-3-2

Abstract

A newly-designed problem-based laboratory experiment utilizing a benchtop NMR spectrometer was implemented for undergraduate students. The aim of the experiment was to have a hands-on, problem-based approach that focused on structure elucidation as well as practical aspects such as sample preparation, data acquisition and manipulation. The experimental protocol also allowed the students to understand other aspects of NMR spectroscopy such as identification of impurities and its application in monitoring reaction progress. Results from a survey and a quiz conducted as part of the study clearly indicated that this hands-on approach not only helped to reinforce the theory learned in a lecture course, but also allow the students to realize the full potential of this important spectroscopic technique.

Keywords:
General and Organic Chemistry NMR Spectroscopy Hands-On Experiment Problem-Based Learning Benchtop NMR Spectrometer

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