World Journal of Chemical Education
ISSN (Print): 2375-1665 ISSN (Online): 2375-1657 Website: http://www.sciepub.com/journal/wjce Editor-in-chief: Prof. V. Jagannadham
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World Journal of Chemical Education. 2016, 4(3), 52-63
DOI: 10.12691/wjce-4-3-2
Open AccessArticle

A Hands-on Problem-Based NMR Experiment using a Benchtop Spectrometer for the Undergraduate Laboratory Supplementary Information (SI)

Jonathan Wong1, Houguang Jeremy Chen1, Ai-Hua Seow1, Susanne D. Riegel2, and Sumod A. Pullarkat1,

1Division of Chemistry and Biological Chemistry, School of Physical & Mathematical Sciences, Nanyang Technological University, Singapore 637371, Singapore

2Application Chemistry, Nanalysis Corp., Calgary, Alberta, Canada

Pub. Date: June 24, 2016

Cite this paper:
Jonathan Wong, Houguang Jeremy Chen, Ai-Hua Seow, Susanne D. Riegel and Sumod A. Pullarkat. A Hands-on Problem-Based NMR Experiment using a Benchtop Spectrometer for the Undergraduate Laboratory Supplementary Information (SI). World Journal of Chemical Education. 2016; 4(3):52-63. doi: 10.12691/wjce-4-3-2

Abstract

A newly-designed problem-based laboratory experiment utilizing a benchtop NMR spectrometer was implemented for undergraduate students. The aim of the experiment was to have a hands-on, problem-based approach that focused on structure elucidation as well as practical aspects such as sample preparation, data acquisition and manipulation. The experimental protocol also allowed the students to understand other aspects of NMR spectroscopy such as identification of impurities and its application in monitoring reaction progress. Results from a survey and a quiz conducted as part of the study clearly indicated that this hands-on approach not only helped to reinforce the theory learned in a lecture course, but also allow the students to realize the full potential of this important spectroscopic technique.

Keywords:
General and Organic Chemistry NMR Spectroscopy Hands-On Experiment Problem-Based Learning Benchtop NMR Spectrometer

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