American Journal of Materials Engineering and Technology
ISSN (Print): 2333-8903 ISSN (Online): 2333-8911 Website: https://www.sciepub.com/journal/materials Editor-in-chief: Serge Samper
Open Access
Journal Browser
Go
American Journal of Materials Engineering and Technology. 2017, 5(1), 14-23
DOI: 10.12691/materials-5-1-3
Open AccessArticle

On the Role of Boride in the Structural Integrity of a Turbine Disc Superalloy’s Solid State Weld

K.M. Oluwasegun1, , J.O Olawale1, M.D. Shittu1, O.O. Ige1, P.O. Atanda1, O.O. Ajide2 and L.O. Osoba3

1Department of Materials Science and Engineering, Obafemi Awolowo University, Ile-Ife, Nigeria

2Department of Mechanical Engineering, University of Ibadan, Nigeria

3Department of Metallurgical and Materials Engineering, University of Lagos, Nigeria

Pub. Date: October 13, 2017

Cite this paper:
K.M. Oluwasegun, J.O Olawale, M.D. Shittu, O.O. Ige, P.O. Atanda, O.O. Ajide and L.O. Osoba. On the Role of Boride in the Structural Integrity of a Turbine Disc Superalloy’s Solid State Weld. American Journal of Materials Engineering and Technology. 2017; 5(1):14-23. doi: 10.12691/materials-5-1-3

Abstract

This work reports the melting of boride precipitates along the grain boundary of a supposedly solid state welding of a polycrystalline superalloy, and discusses its attendant effect on the hot ductility behaviour of the alloy. Nickel-based superalloy used for this study was previously processed by hot extrusion of argon atomized powered followed by forging. The alloy was solution heat treated at 1120 °C, aged at 760 °C and subsequently air cooled to room temperature. Thereafter, it was welded by inertial friction welding (IFW) at a forging pressure of 250 MPa and finally stressed relieved at 760 °C for 8 hours. The microstructures of welded samples were studied by scanning and scanning transmission electron microscopes. Gleeble hot ductility test was carried out on tensile specimen machined from the welded sample. The microstructures of the welded alloy shows that boride precipitates liquated along the grain boundary within the heat affected zone (HAZ) as a result of rapid heating of IFW. The results of hot ductility test revealed that the melting of boride lowered the hot ductility of the alloy. It was concluded that the boride precipitates liquated along the grain boundary of the nickel-based superalloy during solid state welding and lowered its hot ductility.

Keywords:
superalloy solid state welding boride precipitates grain boundary hot ductility welding

Creative CommonsThis work is licensed under a Creative Commons Attribution 4.0 International License. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/

Figures

Figure of 10

References:

[1]  W.C. Hagel, The Superalloys, John Wiley & Sons, New York, 1972.
 
[2]  R.C. Reed, The Superalloys, Fundermentals and Applications, University Press, Cambridge, 2006.
 
[3]  A.F. Padilha, G. Schanz, Precipitation of a boride phase in 15-percent-Cr-15-percent-Ni-Mo-Ti-B austenitic stainless-steel (DIN 1.4970), Journal of Nuclear Materials 95 (1980) 229-238.
 
[4]  C. Stocker, M. Zimmermann, H.J. Christ, Z.L. Zhan, C. Cornet, L.G. Zhao, M.C. Hardy, J. Tong, Microstructural characterisation and constitutive behaviour of alloy RR1000 under fatigue and creep-fatigue loading conditions, Material Science and Engineering A 518 (2009) 27-34.
 
[5]  D.H. Maxwell, J.F. Baldwin, J.F. Radavich, New concept in superalloy ductility, Metallurgia and Metal Forming 42 (1975) 332.
 
[6]  H.R. Zhang, O.A. Ojo, Cr-rich nanosize precipitates in a standard heat-treated Inconel 738 superalloy, Philosophical Magazine 90 (2010) 765-782.
 
[7]  M. Kurban, U. Erb, K.T. Aust, A grain boundary characterization study of boron segregation and carbide precipitation in alloy 304 austenitic stainless steel, Scripta Materialia, 54 (2006) 1053-1058.
 
[8]  W.A. Owczarski, D.S. Duvall, C.P. Sullivan, Model for heat-affected zone cracking in nickel-base superalloys, Welding Journal 45 (1966) 145-155.
 
[9]  M. Prager, C.S. Shira, Welding of precipitation-hardening nickel-base alloys, Welding Research Council - Bulletin Series 128 (1968) 55.
 
[10]  M.H. Haakens, J.H.G. Matthey, New approach to the weldability of nickel-base as-cast and powder metallurgy superalloys, Welding Journal 61 (1982) 25-30.
 
[11]  T.J. Kelly, Welding metallurgy of investment cast nickel-based superalloys, Weldability of Materials 1990 151-157.
 
[12]  O.A. Ojo, R.G. Ding, M.C. Chaturvedi, Heat affected zone microfissuring in a laser beam welded directionally solidified Ni3Al-base alloy, Scripta Materialia 54 (2006) 2131-2136.
 
[13]  G. Cam, M. Kocak, Progress in joining of advanced materials, International Materials Reviews 43 (1998) 1-44.
 
[14]  M.B. Henderson, D. Arrell, M. Larsson, G. Marchant, Nickel based superalloy welding practices for industrial gas turbine applications, Science and Technology of Welding and Joining 9 (2004) 13-21.
 
[15]  J.K. Tien, T.J. Caulfield, Superalloys, Supercomposites and Superceramics, Academic Press Inc, London, 1989.
 
[16]  Z.W. Huang, H.Y.Li, M. Preuss, M. Karadge, P. Bowen, S. Bray, G. Baxter, Inertia friction welding dissimilar nickel-based superalloys alloy 720Li to IN718, Metallurgical and Materials Transactions A – Physical Metallurgy and Materials Science 38A (2007) 1608-1620.
 
[17]  M. Preuss, J.W.L. Pang, P.J. Withers, G.J. Baxter, Inertia welding nickel-based superalloy: Part II. Residual stress characterization, Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science 33 (2002) 3227-3234.
 
[18]  F. Tancret, Thermo-Calc and Dictra simulation of constitutional liquation of gamma prime (γ') during welding of Ni base superalloys, Computational Materials Science 41 (2007) 13-19.
 
[19]  K.M. Oluwasegun, J.O. Olawale, O.O. Ige, M.D. Shittu, A.A. Adeleke, B.O. Malomo, Microstructural characterization of thermomechanical and heat-affected zones of an inertia friction welded astroloy, Journal of Materials Engineering and Performance 23 (2014) 2834-2846.
 
[20]  R.K. Sidhu, O.A. Ojo, M.C. Chaturvedi, Microstructural analysis of laser-beam-welded directionally solidified Inconel 738, Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science 38 (2007) 858-870.
 
[21]  L. Wang, M. Preuss, P.J. Withers, G. Baxter, P. Wilson, Energy-input-based finite-element process modeling of inertia welding, Metallurgical and Materials Transactions B: Process Metallurgy and Materials Processing Science 36 (2005) 513-523.
 
[22]  H.A. Shahsavari, A.H. Kokabi, S. Nategh, Effect of preweld microstructure on HAZ liquation cracking of Rene 80 superalloy, Materials Science and Technology 23 (2007) 547-555.
 
[23]  R.K. Sidhu, O.A. Ojo, M.C. Chaturvedi, Microstructural response of directionally solidified Rene 80 superalloy to gas-tungsten arc welding, Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science 40 (2009) 150-162.
 
[24]  O.A. Ojo, N.L. Richards, M.C. Chaturvedi, Study of the fusion zone and heat affected zone microstructures in tungsten inert gas-welded INCONEL 738LC superalloy, Metallurgical and Materials Transactions A – Physical Metallurgy and Materials Science 37A (2006) 421-433.
 
[25]  P. Villars, A. Prince, H.Okamoto, Handbook of Ternary Alloy Phase Diagram 5 (1995) 5526.
 
[26]  O.A. Ojo, M.C. Chaturvedi, On the role of liquatedγ' precipitates in weld heat affected zone microfissuring of a nickel-based superalloy, Materials Science and Engineering A – Structural Materials Properties Microstructure and Processing 403 (2005). 77-86.
 
[27]  W. Lin, J.C. Lippold, W.A. Baeslack, An evaluation of heat-affected zone liquation cracking susceptibility.1. Development of a method for quantification, Welding Journal 72 (1993) 135-153.