World Journal of Chemical Education
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World Journal of Chemical Education. 2021, 9(2), 50-56
DOI: 10.12691/wjce-9-2-3
Open AccessArticle

An Innovative Method Designed for the Synthesis of Some New Mixed Ligand Ni(II) Complexes Its Characterization and Applications

Jitendra M. Pawara1, and Sunil S. Patil1

1Department of Chemistry, Changu Kana Thakur Arts Commerce and Science College (Autonomous), New Panvel, Maharashtra, India

Pub. Date: May 15, 2021

Cite this paper:
Jitendra M. Pawara and Sunil S. Patil. An Innovative Method Designed for the Synthesis of Some New Mixed Ligand Ni(II) Complexes Its Characterization and Applications. World Journal of Chemical Education. 2021; 9(2):50-56. doi: 10.12691/wjce-9-2-3

Abstract

In the present work, a series of new mixed ligand Ni(II) complexes of the type [Ni(P)(L).2H2O] have been synthesized by using 2-amino-6-methyl pyrimidine-4-ol (HP), a primary ligand and N- and O- donor amino acids (HL) secondary ligands. Synthesis of Ni(II) complexes has been carried out by thermal and microwave methods. Results show that complexes synthesized by the microwave method were more efficient than the thermal method. Preparation time in the microwave method was short (4-7 min.) as compared to the thermal method (45 min.). Additionally, the microwave technique gave a very high yield (90%) of the complexes. The prepared complexes were characterized by Gouy experiment, FTIR, elemental analysis, TGA, and DTA at room temperature. The complexes have shown considerable antimicrobial activities such as antifungal and antibacterial activity.

Keywords:
Ni(II) complexes 2-amino-6-methyl pyridine-4-ol amino acids microwave antimicrobial activity

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